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A Cummins ISB 5.9 liter medium-duty engine with cooled EGR has been used to study an early extrusion of an advanced ceramic uncatalyzed diesel particulate filter (DPF). Data for the advanced ceramic material (ACM) and an uncatalyzed cordierite filter of similar dimensions are presented. Pressure drop data as a function of mass loadings (0, 4, and 6 grams of particulate matter (PM) per liter of filter volume) for various flow rate/temperature combinations (0.115 - 0.187 kg/sec and 240 - 375 °C) based upon loads of 15, 25, 40 and 60% of full engine load (684 N-m) at 2300 rpm are presented. The data obtained from these experiments were used to calibrate the MTU 1-D 2-Layer computer model developed previously at MTU. Clean wall permeability determined from the model calibration for the ACM was 5.0e-13 m2 as compared to 3.0e-13 m2 for cordierite.

Steady state loading characterization experiments were conducted at three different engine load conditions and rated speed on the cracked catalyzed particulate filter (CPF). The experiments were performed using a 10.8 L 2002 Cummins ISM-330 heavy duty diesel engine. The CPF underwent a ring off failure, commonly seen in particulate filters, due to high radial and axial temperature gradients. The filters were cracked during baking in an oven which was done to regenerate PM collected after every loading characterization experiment. Two different configurations i.e. with and without a diesel oxidation catalyst (DOC) upstream of the CPF were studied. The data were compared with that on an un-cracked CPF at similar engine conditions and configurations. Pressure drop, transient filtration efficiency by particle size and PM mass and gaseous emissions measurements were made during each experiment.

Steady-state particulate loading experiments were conducted on an advanced production catalyzed particulate filter (CPF), both with and without a diesel oxidation catalyst (DOC). A heavy-duty diesel engine was used for this study with the experiments conducted at 20, 40, 60 and 75 % of full load (1120 Nm) at rated speed (2100 rpm). The data obtained from these experiments were used and are necessary for calibrating the MTU 1-D 2-Layer CPF model. These experimental and modeling results were compared to previous research conducted at MTU that used the same engine but an earlier development version of the combination of DOC and CPF. The motivation for the comparison of the two systems was to determine whether the reformulated production catalysts performed as good or better than the early development catalysts. The results were compared to understand the filtration and oxidation differences between the two DOC+CPF and the CPF-only aftertreatment systems.

The catalyzed particulate filter (CPF), used in conjunction with a diesel oxidation catalyst (DOC) is an important aftertreatment device used to meet Environmental Protection Agency (EPA) heavy-duty diesel emission standards for particulate matter (PM). Numerical modeling of these exhaust after-treatment devices decreases the time and cost of development involved. Modeling CPF active regeneration gives insight into the PM oxidation kinetics, which helps in reducing the regeneration fuel penalty. As seen from experimental data, active regeneration of the CPF results in a significant temperature increase into the CPF (up to 8°C/sec) which affects the oxidation rate of particulate matter (PM). PM oxidation during active regeneration was determined to be a function of filter PM loading, inlet temperature and inlet hydrocarbon concentration.

A 2-dimensional numerical model (MTU-FILTER) for a single channel of a honeycomb ceramic diesel particulate trap has been developed. The mathematical modeling of the filtration, flow, heat transfer and regeneration behavior of the particulate trap is described. Numerical results for the pressure drop and particulate mass were compared with existing experimental results. Parametric studies of the diesel particulate trap were carried out. The effects of trap size and inlet temperature on the trap performance are studied using the trap model. An approximate 2-dimensional analytical solution to the simplified Navier-Stokes equations was used to calculate the velocity field of the exhaust flow in the inlet and outlet channels. Assuming a similarity velocity profile in the channels, the 2-dimensional Navier-Stokes equations are approximated by 1-dimenisonal conservation equations, which is similar to those first developed by Bissett.

A study was conducted to assess the effects of a water-diesel fuel emulsion with and without an oxidation catalytic converter (OCC) on steady-state heavy-duty diesel engine emissions. Two OCCs with different metal loading levels were used in this study. A 1988 Cummins L10-300 heavy-duty diesel engine was operated at the rated speed of 1900 rpm and at 75% and 25% load conditions (EPA modes 9 and 11 respectively) of the 13 mode steady-state test as well as at idle. Raw exhaust emissions' measurements included total hydrocarbons (HC), oxides of nitrogen (NOx) and nitric oxide (NO). Diluted exhaust measurements included total particulate matter (TPM) and its primary constituents, the soluble organic (SOF), sulfate (SO42-) and the carbonaceous solids (SOL) fractions. Vapor phase organic compounds (XOC) were also analyzed. The SOF and XOC samples were analyzed for selected polynuclear aromatic hydrocarbons (PAHs).

The effects of an oxidation catalytic converter (OCC), an emulsified fuel, and their combined effects on particle number and volume concentrations compared to those obtained when using a basefuel were studied. Particle size and particulate emission measurements were conducted at three operating conditions; idle (850 rpm, 35 Nm), Mode 11 (1900 rpm, 277 Nm) and Mode 9 (1900 rpm, 831 Nm) of the EPA 13 mode cycle. The individual effects of the emulsified fuel and the OCC as well as their combined effects on particle number and volume concentrations were studied at two different particle size ranges; the nuclei (less than or equal to 50 nm) and accumulation (greater than 50 nm) modes. An OCC loaded with 10 g/ft3 platinum metal (OCC1) and a 20% emulsified fuel were used for this study and a notable influence on the particle size with respect to number and volume distributions was observed.

A numerical model to simulate the filtration and oxidation of PM as well as the oxidation of NO, CO and HC in a CPF was developed in reference [1]. The model consists of parameters related to filtration and oxidation of PM and oxidation of NO, CO and HC. One of the goals of this paper is to use the model to determine the PM and gaseous species kinetics for ULSD, B10 and B20 fuels using data from passive oxidation and active regeneration engine experimental studies. A calibration procedure to identify the PM cake and wall filtration parameters and kinetic parameters for the PM oxidation and NO, CO and HC oxidation was developed. The procedure was then used with the passive oxidation [2] and active regeneration [3] engine data. The tests were conducted on a 2007 Cummins ISL engine with a DOC and CPF aftertreatment system. The simulation results show good agreement with the experimental CPF pressure drop, PM mass retained measurements and the outlet NO, NO2, CO and HC concentrations.

Diesel particulate matter in both the diluted and undiluted state is subject to the processes of coagulation, condensation or evaporation, and nucleation which causes continuous changes in its physical characteristics. The Electrical Aerosol Analyzer (EAA) is used to measure the diesel particle size distribution in the MTU dilution tunnel for a naturally aspirated direct-injection diesel engine operated on the EPA 13 mode cycle. The design and development of accurate and repeatable sampling methods using the EAA are presented. These methods involve both steady-state tunnel and bag measurements. The data indicate a bimodal nature within the 0.001 to 1 μm range. The first mode termed the “embroynic mode” has a saddle point between 0.005 to 0.015 μm and the second mode termed the “aggregation mode” lies between .08 to .15 μm for the number distribution.

The passive oxidation of particulate matter (PM) in a diesel catalyzed particulate filter (CPF) was investigated in a series of experiments performed on two engines. A total of ten tests were completed on a 2002 Cummins 246 kW (330 hp) ISM and a 2007 Cummins 272 kW (365 hp) ISL. Five tests were performed on each engine to determine if using engine technologies certified to different emissions regulations has an impact on the passive oxidation characteristics of the PM. A new experimental procedure for passive oxidation testing was developed and implemented for the experiments. In order to investigate the parameters of interest, the engines were initially operated at a steady state loading condition where the PM concentrations, flow rates, and temperatures were such that the accumulation of PM within the CPF was obtained in a controlled manner. This engine operating condition was maintained until a CPF PM loading of 2.2 ±0.2 g/L was obtained.

The diesel engine emits exhaust particles that pose a unique set of measurement requirements. To document the state-of-the-art of measurement technology and to improve measurement quality, the Smoke and Particulate Panel of the Diesel Exhaust Composition group of the Coordinating Research Council reviewed published literature and particulate-sampling data generated by panel members to identify (1) the effects of key sampling parameters on measured particulate mass, (2) the causes of measurement variability, (3) the effects of dilution system design on particulate mass measurement, and (4) promising real-time mass measurement methods. The panel found greater measurement difficulty associated with particulates than for gaseous pollutants because of engine-produced variations, the sensitivity of measured particulate mass to dilution parameters, and random errors in the independent measurements which comprise a particulate measurement.

Analytical ferrography was used as a wear measurement tool while implimenting a procedure to calculate the wear particle generation rate and filter efficiency during laboratory diesel engine testing. The engine testing methodology with quantitative ferrography proved to be a sensitive wear measurement technique in detecting a reduction in the wear particle generation rate for a better anti-wear (API SF/CD) oil from that of a baseline API SD/CD oil. Ferrography and spectroscopy were useful as diagnostic tools for the detection and correction of the unexpected circulation of copper contaminant in the lubrication system. A journal bearing failure was detected with qualitative ferrography and verified with an engine teardown while spectroscopy did not detect the bearing failure.

One of the more objectionable aspects of the use of diesel engines has been the emission of particulate matter. A literature review of combustion flames, theoretical calculations and dilution tunnel experiments have been performed to elucidate the chemical and physical processes involved in the formation of diesel particulate matter. A comparative dilution tunnel study of diluted and undiluted total particulate data provided evidence supporting calculations that indicate hydro-carbon condensation should occur in the tunnel at low exhaust temperatures. The sample collection system for the measurement of total particulate matter and soluble sulfate in particulate matter on the EPA 13 mode cycle is presented. A method to correct for hydrocarbon interferences in the EPA barium chloranilate method for the determination of sulfate in particulate matter is discussed.

This paper is concerned with the demonstration of a methodology for chemically characterizing diesel particulate organic matter (POM) emissions. The procedure begins with a Soxhlet extraction of the POM with dichloromethane to obtain a soluble organic fraction (SOF). The acidic and basic portions of the SOF are isolated by liquid-liquid extraction techniques with aqueous base and aqueous acid, respectively. The neutral portion of the extract is separated into paraffin, aromatic, transitional and oxygenated fractions by column chromatography on silica gel. Two additional fractions, the ether insoluble and hexane insoluble fractions, are also separated by the procedure. Quantitative mass data are presented on the extraction and fractionation of twelve particulate samples from the exhaust of a medium-duty diesel engine collected in a dilution tunnel at a volume dilution ratio of 8 to 1.

Formation of pollutants from diesel combustion and methods for their control have been reviewed. Of these methods, fuel injection rate and timing were selected for a parametric study relative to total particulate, soluble organic fraction (SOF), sulfates, solids and NO and NO2 emissions from a heavy-duty, turbocharged, after-cooled, direct-injection (DI) diesel. Chemical analyses of the SOF were performed at selected engine conditions to determine the effects of injection rate and timing on each of the eight chemical subfractions comprising the SOF. Biological character of the SOF was determined using the Ames Salmonella/microsome bioassay.

The objective of this research was to obtain diesel particle size distributions from a 1988 and a 1991 diesel engine using three different fuels and two exhaust control technologies (a ceramic particle trap and an oxidation catalytic converter). The particle size distributions from both engines were used to develop models to estimate the composition of the individual size particles. Nucleation theory of the H2O and H2SO4 vapor is used to predict when nuclei-mode particles will form in the dilution tunnel. Combining the theory with the experimental data, the conditions necessary in the dilution tunnel for particle formation are predicted. The paper also contains a discussion on the differences between the 1988 and 1991 engine's particle size distributions. The results indicated that nuclei mode particles (0.0075-0.046 μm) are formed in the dilution tunnel and consist of more than 80% H2O-H2SO4 particles when using the 1988 engine and 0.29 wt% sulfur fuel.

Diesel exhaust particle size distributions were measured using an Electrical Aerosol Analyzer (EAA) with both conventional (0.31 wt. pet sulfur) and low sulfur fuel (0.01 wt pet sulfur) with and without a ceramic diesel particle filter (DPF). The engine used for this study was a 1988 heavy-duty diesel engine (Cummins LTA10-300) operated at EPA steady-state modes 9 and 11. The particle size distribution results indicated the typical bi-modal distribution; however, there were clear differences in the number of particles in each mode for all conditions. For the baseline conditions with no DPF, there was more than one order of magnitude greater number of particles in the nuclei mode for the conventional fuel as compared to the low sulfur fuel, while the accumulation modes for each fuel were nearly identical.

A study has been made of piston ring wear and total engine wear using literature data and new experimental results. The main purpose of the study was to establish the effects of oil and coolant temperatures on engine wear. Wear trends that were found in the early 1960's may not be valid any longer because of the development of higher BMEP turbocharged diesel engines, better metallurgical wear surfaces and improved lube oil properties. New data are presented for the purpose of describing present wear trends. A direct-injection, 4-cycle, turbocharged diesel engine was used for the wear tests. The radioactive tracer technique was used to measure the top piston ring chrome face wear. Atomic emission spectroscopy was employed to determine the concentration of wear metals in the oil to determine total engine wear based on iron and lead. The data were analyzed and compared to the results found in the literature from previous investigators.

Exhaust emissions were characterized from a Cummins LTA10 heavy-duty diesel engine operated at two EPA steady-state modes with and without an uncatalyzed Corning ceramic particulate trap. The regulated emissions of nitrogen oxides (NOx), hydrocarbons (HC), and total particulate matter (TPM) and its components as well as the unregulated emissions of PAH, nitro-PAH, mutagenic activity and particle size distributions were measured. The consistently significant effects of the trap on regulated emissions included reductions of TPM and TPM-associated components. There were no changes in NOx and HC were reduced only at one operating condition. Particle size distribution measurements showed that nuclei-mode particles were formed downstream of the trap, which effectively removed accumulation-mode particles. All of the mutagenicity was direct-acting and the mutagenic activity of the XOC was approximately equivalent to that of the SOF without the trap.

A study of the Corning ceramic diesel particulate trap was conducted to investigate the trap's overall effect on diesel particulate fractions (soluble organic fraction. SOF; solid fraction, SOL; and sulfate fraction. SO4) under four different engine loads at 1680 rpm. The trap was found to filter the SOL fraction most efficiently with the SOF and SO4 fraction following in respective order. The filter efficiency of all fractions increased with increasing engine load. Graphs illustrating filter efficiency versus engine load indicate the slope of the SOF filter efficiency was smaller in magnitude than the TPM and SOL and SO4, fractions, which had similar slopes. The different slope of the SOF filter efficiency indicates other influences may be involved with the reduction in the SOF through the trap. Particle size distribution measurements in diluted exhaust revealed particle formation downstream of the trap.